Chemistry Labs

Organic chemistry

Pyridine, indole, furan, thiophene

Aromatic heterocycles replace one or more carbon atoms of a benzene-like ring by heteroatoms, changing basicity, electron distribution and reactivity.

IntuitionIntuition: a ring with a personality

Replace one ring carbon of benzene by nitrogen and the ring no longer shares its electron cloud evenly. In pyridine the nitrogen lone pair stays outside the π system and is available for bonding to protons, while in furan one oxygen lone pair contributes to the aromatic sextet and is much less basic.

Pyridine, furan, thiophene and indole are drawn from ring geometry and bond order; rotate to inspect their planar π systems.

SchoolSchool level: names, formulas and typical examples

Definition:

A ring compound whose ring contains atoms other than carbon, commonly nitrogen, oxygen or sulfur. Aromatic heterocycles satisfy a conjugated, cyclic π system that gives unusual stability.

Pyridine is a six-membered C₅H₅N ring that acts like an aza-benzene. Indole is benzene fused to pyrrole and is the scaffold of tryptophan, serotonin and many dyes. Furan and thiophene are five-membered oxygen- and sulfur-containing rings that are electron rich relative to benzene.

Selected aromatic heterocycles
RingFormulaMain feature
PyridineC₅H₅NBasic N lone pair; coordinate donor
IndoleC₈H₇NBenzene fused to pyrrole; electron rich
FuranC₄H₄OO lone pair contributes to aromaticity
ThiopheneC₄H₄SMore benzene-like than furan

UndergraduateUniversity: electron distribution and electrophilic substitution

In pyridine, electronegative nitrogen withdraws π electron density, making the ring less reactive toward electrophilic aromatic substitution than benzene and most reactive at the 3-position. In furan, thiophene, pyrrole and indole the heteroatom donates electron density into the ring; these rings are electron rich and substitution patterns differ by position and heteroatom.

CX5HX5N+HX+→CX5HX5NHX+pKa(CX5HX5NHX+)≈5.2\ce{C5H5N + H+ -> C5H5NH+}\qquad pK_a(\ce{C5H5NH+}) \approx 5.2

Example: Explain relative basicity

Pyridine is a much stronger base than pyrrole. Why does the nitrogen lone pair accept a proton more readily in pyridine?

Solution

In pyridine the N lone pair occupies an in-plane sp² orbital that does not take part in the aromatic sextet, so protonation does not destroy aromaticity. In pyrrole the lone pair is part of the π sextet; protonation would remove aromatic stabilization.

References

  • Heterocyclic Chemistry (5th ed.) · John A. Joule, Keith Mills, 2010